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560137 - ČSN EN 16924 - Potraviny - Stanovení zearalenonu v jedlých rostlinných olejích metodou LC-FLD nebo LC-MS/MS | ||
Název : 560137 - ČSN EN 16924 - Potraviny - Stanovení zearalenonu v jedlých rostlinných olejích metodou LC-FLD nebo LC-MS/MS
Označení normy : ČSN EN 16924 Katalogové číslo : 503376 Třídící znak : 560137 Účinnost : 2018-12-01 Věstník : 2018.11 Strany : 36 Převzata :vyhlášením ve Věstníku - v angličtině | ||
Cena : | 340.00 Kč (DPH= 0%), s DPH= 340.00 Kč | |
ANOTACE "ČSN EN 16924 This European Standard describes a procedure for the determination of the zearalenone content in edible vegetable oils specifically maize germ oil by either of the following techniques: High performance liquid chromatography with fluorescence detection (LC-FLD) or high performance liquid chromatography with tandem mass spectrometry (LC-MS/MS) after basic extraction of the diluted oil. The method has been validated for zearalenone in naturally contaminated maize germ oil at levels of 61,2 µg/kg to 515 µg/kg [5]. Laboratory experiences [6] have shown that this method is also applicable to other vegetable oils such as wheat germ oil (n = 4), sunflower oil (n = 5), pumpkin seed oil (n = 1), soybean oil (n = 5), hemp seed oil (n = 5), rape seed oil (n = 11), and mixed oils including maize germ oil (n = 3). However occasionally, samples can result in interferences in the FLD-chromatograms. In this case, the detection with MS/MS is recommended." |